lamp black

Turkey
18th Century
Source: Unsalan, O., Oten, A., & Yaman, B. (2021). Crystallite size of the graphitic phase in soot ink based on historic recipe: A potential dating tool for old manuscripts. Research Square. https://doi.org/10.21203/rs.3.rs-1211962/v1
Recipe Details

Ingredients

soot, lamp black

Evidence

"Our findings demonstrated that black paint... was consistent with the database-matched lamp black by 82.27% hit score."

Remarks

The pigment was identified by Raman spectral data showing sp3 and sp2 hybridised amorphous carbon FWHM at D and G bands at 1384 and 1609 cm-1 (p. 3). The absence of a phosphate band at 960 cm-1 specifically confirms that the pigment is not bone black or ivory black (p. 3). The crystallite size was determined to be 24.33 nm using the ID/IG intensity ratio of 0.79 (p. 4). FWHM values for the D and G bands were 101.01 and 213.95 cm-1 respectively (Table 1, p. 5).

Scientific Analysis
Chemical CompositionC
Analytical Techniques
Raman
Certainty Level
Confirmed
Instrumentally Verified
Verified
Metadata
Material Type
pigment
ColorBlack
RegionTurkey
Approx. Year1750
Source Information
AuthorUnsalan, O., Oten, A., & Yaman, B.
Collectionsoot from oil lamps
Language
N/A
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