lac dye
Andalusia
12th Century
Source: Vieira, M., Nabais, P., Angelin, E. M., Araújo, R., Almeida Lopes, J., Martín García, L., & Melo, M. J. (2019). Organic red colorants in Islamic manuscripts (12th-15th c.) produced in al-Andalus, part 1. Dyes and Pigments, 166, 451-459.
Recipe Details
Ingredients
lac, sticklac, borax, sodium carbonate, ashes
Preparation Steps
Based on the Ibn Bādġs manuscript (c. 1025), the recipe 'red ruby from the lukk' (Chapter 6) involves grinding the resin (sticklac) and adding a basic solution. The mixture is filtered to remove impurities and residual resin. For this specific Koran formulation, the recipe adds borax and sodium carbonate derived from ashes to the water; notably, no alum is used as a complexing agent (p. 4).
Original Recipe Text
Based on the Ibn Bādġs manuscript (c. 1025), the recipe 'red ruby from the lukk' (Chapter 6) involves grinding the resin (sticklac) and adding a basic solution. The mixture is filtered to remove impurities and residual resin. For this specific Koran formulation, the recipe adds borax and sodium carbonate derived from ashes to the water; notably, no alum is used as a complexing agent (p. 4).
Evidence
"Microspectrofluorimetry detected the presence of a lac dye chromophore in all the manuscripts studied and ascribed it to specific medieval recipes for three of the manuscripts. This was based on the very good matches obtained with our database of paint reconstructions... the dark reds found in the Koran compared very well with the recipe ‘to make red ruby from lukk’ from Ibn Bādġs text (11th c.)"
Remarks
The Koran manuscript (1198) contains only traces of its original illumination. Infrared spectroscopy (microFTIR) identified a proteinaceous binder combined with shellac resin, the latter confirmed by the presence of erythrolaccin (max at 474 nm) via microspectrofluorimetry (p. 5, 8).
Scientific Analysis
Chemical Compositionlaccaic acids
Analytical Techniques
microspectrofluorimetry
FTIR
XRF
fibre optic reflectance spectroscopy (FORS-VIS)
Certainty Level
Confirmed
Instrumentally Verified
Verified
Metadata
Material Type
pigment
BinderLac resin
Paper TypeParchment
ColorRed
RegionAndalusia
Approx. Year1150
Source Information
AuthorVieira, M., Nabais, P., Angelin, E. M., Araújo, R., Almeida Lopes, J., Martín García, L., & Melo, M. J.
CollectionKoran (1198), Fondo Ka'ti
Language
N/A
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