cotton fibers

Egypt
14th Century
Source: Taha, A. S. (2024). Evaluation The Condition of Historical Manuscript" Al-MUTAWIL by Al-Qazwini " from the 14th Century AD is kept in Egypt's (Al – Azhar library): A Case Study. SHEDET, (12), 378-397.
Recipe Details

Ingredients

cotton fibers, kaolinite, calcium carbonate, calcite

Preparation Steps

The paper was manufactured from rags consisting of linear long cellulose fibers (p. 379). Analysis confirmed the specific source of these fibers as cotton (p. 382). During production, fillers and coating materials were added to enhance mechanical qualities. Mineral fillers identified through elemental analysis include kaolinite (Al2Si2O5(OH)4) and calcium carbonate (CaCO3) (p. 383). The high presence of aluminum and silicon specifically suggests the use of kaolinite, while high calcium levels point to calcium carbonate or calcite crystals (p. 383).

Original Recipe Text

The paper was manufactured from rags consisting of linear long cellulose fibers (p. 379). Analysis confirmed the specific source of these fibers as cotton (p. 382). During production, fillers and coating materials were added to enhance mechanical qualities. Mineral fillers identified through elemental analysis include kaolinite (Al2Si2O5(OH)4) and calcium carbonate (CaCO3) (p. 383). The high presence of aluminum and silicon specifically suggests the use of kaolinite, while high calcium levels point to calcium carbonate or calcite crystals (p. 383).

Evidence

"morphological analysis revealed that goat skin was used in making leather for bookbinding, and cotton was used to produce paper."

Remarks

The manuscript is described as severely damaged, suffering from disintegration, erosion, and biological attack (p. 380). The paper has reached an acidic state with a pH of 4.5, which is identified as a critical factor in the breakdown of cellulose chains through acid hydrolysis (p. 391). XRD analysis showed a decline in the crystallinity index, indicating significant chemical and mechanical alteration of the cellulose molecules over time (p. 392). Elemental mapping showed spots influenced by iron and aluminum (p. 382).

Scientific Analysis
Analytical Techniques
SEM-EDAX
FTIR
X-ray diffraction
pH measurement
Certainty Level
Confirmed
Instrumentally Verified
Verified
Metadata
Material Type
paper
Paper Typecotton fibers
ColorWhite
RegionEgypt
Approx. Year1350
AI Suggestions
Find similar recipes based on ingredients and preparation methods.
    cotton fibers (14th Century) | Islamic Ink Atlas