iron-gall ink with no significant impurities
Egypt
9th Century
Source: Sathiyamani, S., Fedeli, A., Marotta, G. & Colini, C. (2025). From fragments to text and ink: a scientific and historical study of an Umayyad Qur’ān. npj Heritage Science, 13:478.
Recipe Details
Ingredients
iron filings, nails, tannins, gum arabic
Preparation Steps
Described as a secondary ink, likely a non-vitriolic iron-gall ink (p. 4). It is characterized by a high iron content but a lack of copper, manganese, or zinc impurities (p. 4, 6). Such inks are known from historical Arabic recipes that specify the use of iron filings, nails, or solid pieces of iron rather than vitriol (p. 4). Like the primary ink, it contains gum arabic as a binder (p. 7).
Original Recipe Text
Described as a secondary ink, likely a non-vitriolic iron-gall ink (p. 4). It is characterized by a high iron content but a lack of copper, manganese, or zinc impurities (p. 4, 6). Such inks are known from historical Arabic recipes that specify the use of iron filings, nails, or solid pieces of iron rather than vitriol (p. 4). Like the primary ink, it contains gum arabic as a binder (p. 7).
Evidence
"XRF scans, displayed as heat maps in Fig. 7, show the presence of iron in this ink, while contributions from copper, although faint, can be attributed to the text written on the verso, suggesting the use of an iron-gall ink with no significant impurities or even of a non-vitriolic iron-gall ink for the reinking."
Remarks
This secondary ink was used for later scribal interventions, specifically re-inking (jandara) faded text on fragments Hs. 15a and Hs. 15c, and inserting a correction on Hs. 15b (p. 1, 9, 10). The practice of re-inking was considered a pious act to maintain the legibility of the sacred text (p. 10). The study suggests these interventions occurred when the manuscript was endowed to the mosque of 'Amr b. al-'As after 876-9 CE (p. 10).
Scientific Analysis
Chemical CompositionFe, K
Analytical Techniques
XRF
FTIR
Digital microscopy
Certainty Level
Probable
Instrumentally Verified
Verified
Metadata
Material Type
ink
BinderAcacia gum
Paper TypeParchment
ColorBrown
RegionEgypt
Approx. Year850
Source Information
AuthorSathiyamani, S., Fedeli, A., Marotta, G. & Colini, C.
CollectionEgypt
Language
N/A
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