Soot and vitriol

Persia
16th Century
Source: Zekrgoo, Sadra. "Methods of Creating, Testing and Identifying Traditional Black Persian Inks." Restaurator. International Journal for the Preservation of Library and Archival Material 35, no. 2 (2014): 133-158.
Recipe Details

Ingredients

soot, vitriol, gall, gum Arabic powder

Preparation Steps

Ingredients (Recipe 3.I): 1g soot, 1g vitriol, 2g gall, 4g gum Arabic powder. Hot water is added to gum Arabic, stirred, and added to soot to bray. Separately, galls are weighed, broken, boiled, and filtered. The gall water is added to the soot-gum mortar while braying. Finally, vitriol is added and the braying and whipping process is repeated. The ink is bottled and shaken (p. 138).

Original Recipe Text

Ingredients (Recipe 3.I): 1g soot, 1g vitriol, 2g gall, 4g gum Arabic powder. Hot water is added to gum Arabic, stirred, and added to soot to bray. Separately, galls are weighed, broken, boiled, and filtered. The gall water is added to the soot-gum mortar while braying. Finally, vitriol is added and the braying and whipping process is repeated. The ink is bottled and shaken (p. 138).

Evidence

"The Persians... managed to create a new type of ink by integrating the two together. ... The first appearance of this ink dates back to the tenth century where Ibn Muqla Farsi (d. 930) added carbon to the common iron gall ink."

Remarks

This ink combines the stability of carbon with the penetration of iron gall. It appeared maroon under FCIR (p. 151). It was very hard to remove through mechanical means and is very stable in contact with water (p. 152).

Scientific Analysis
Analytical Techniques
FCIR
cross-section-analysis
SEM-EDX
Certainty Level
Confirmed
Instrumentally Verified
Verified
Metadata
Material Type
ink
BinderAcacia gum
Paper TypeZerkall 145 m GSM European acid free mould made paper
ColorPurple
RegionPersia
Approx. Year1550
Source Information
AuthorZekrgoo, Sadra. "Methods of Creating, Testing and Identifying Traditional Black Persian Inks." Restaurator. International Journal for the Preservation of Library and Archival Material 35, no. 2
CollectionTehran, Iran
Language
N/A
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